(E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

Base Information

Chemical Name:(E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide
CAS No.:134896-05-2
Molecular Formula:C₁₇H₁₇NO₆
Molecular Weight:331.325
Hs Code.:

Synonyms:(E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

Suppliers and Price of (E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

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Technology Process of (E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

There total 3 articles about (E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 50906-12-2
4-acetoxy-3-methoxycinnamoyl chloride

: 82659-07-2
2-amino-3-hydroxy-2-cyclopenten-1-one hydrochloride

: 134896-05-2
(E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

Guidance literature:: With pyridine; dmap; at 23 ℃; for 24h;
DOI:10.1080/00397919108016756

Reference yield:

: 1135-24-6,537-98-4
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 134896-05-2
(E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / DMAP, pyridine / 4.5 h / 23 °C

2: oxalyl chloride, DMF / CH₂Cl₂ / 3.5 h / 0 - 23 °C

3: 50 percent / DMAP, pyridine / 24 h / 23 °C

With pyridine; dmap; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1080/00397919108016756

Reference yield:

: 2596-47-6,147677-05-2,34749-55-8
(E)-3-(4-acetoxy-3-methoxyphenyl)acrylic acid

: 134896-05-2
(E)-N-(3-hydroxy-1-oxocyclopent-2-en-2-yl)-3-<4-(acetyloxy)-3-methoxyphenyl> propenamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 3.5 h / 0 - 23 °C

2: 50 percent / DMAP, pyridine / 24 h / 23 °C

With pyridine; dmap; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1080/00397919108016756