3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol

Base Information

Chemical Name:3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol
CAS No.:106543-53-7
Molecular Formula:C₂₁H₂₆O₆
Molecular Weight:374.434
Hs Code.:

Synonyms:3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol

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Chemical Property of 3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol

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Technology Process of 3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol

There total 7 articles about 3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: methyl 3-<2-(3,4-dimethoxyphenyl)-7-methoxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl>propanoate

: 106543-53-7
3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; for 4h; Ambient temperature;

Reference yield:

: 2309-07-1
Methyl ferulate

: 106543-53-7
3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / Ag₂O / benzene; acetone

2: 75 percent / K₂CO₃

3: 81 percent / H₂ / 5percent Pd/C / acetone / 0.33 h / 3102.97 Torr

4: 56 percent / LiAlH₄

With lithium aluminium tetrahydride; hydrogen; potassium carbonate; silver(l) oxide; 5percent Pd/C; In acetone; benzene;
DOI:10.1021/np0103968

Reference yield:

: methyl (E)-3-<2-(3,4-dimethoxyphenyl)-7-methoxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl>prop-2-enoate

: 106543-53-7
3-<(2RS,3SR)-2-(3,4-Dimethoxyphenyl)-2,3-dihydro-3-(hydroxymethyl)-7-methoxybenzofuran-5-yl>-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / H₂ / 5percent Pd/C / acetone / 0.33 h / 3102.97 Torr

2: 56 percent / LiAlH₄

With lithium aluminium tetrahydride; hydrogen; 5percent Pd/C; In acetone;
DOI:10.1021/np0103968