Technology Process of Benzylamine der
There total 6 articles about Benzylamine der which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-chloro-benzonitrile;
With
[2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]triethylphosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; diethylphenylsilane;
at 20 ℃;
for 18h;
Glovebox;
Inert atmosphere;
With
hydrogenchloride;
In
diethyl ether;
at 20 ℃;
for 1h;
Glovebox;
Inert atmosphere;
DOI:10.1055/s-0036-1588441
- Guidance literature:
-
3-chlorobenzamide;
With
[(aNHC)KN(SiMe3)2]2; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane;
In
toluene;
at 40 ℃;
for 12h;
Inert atmosphere;
Glovebox;
Schlenk technique;
With
water; sodium hydroxide;
In
diethyl ether; toluene;
at 40 ℃;
for 1h;
Inert atmosphere;
Glovebox;
Schlenk technique;
With
hydrogenchloride;
In
diethyl ether; water;
Inert atmosphere;
Glovebox;
Schlenk technique;
DOI:10.1039/c9sc05953a
- Guidance literature:
-
1-(3-chlorobenzyl)-3,4-diphenyl-1H-pyrrole-2,5-dione;
With
potassium hydroxide;
In
ethanol; water;
at 102 ℃;
for 0.133333h;
Microwave irradiation;
Green chemistry;
With
hydrogenchloride;
In
ethanol; water;
pH=4;
Temperature;
Green chemistry;
DOI:10.1039/c6gc01318j