phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

Base Information

Chemical Name:phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester
CAS No.:288089-42-9
Molecular Formula:C₅₃H₆₇O₈PSi₃
Molecular Weight:947.34
Hs Code.:

phosphoric acid bis-[3-(<i>tert</i>-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

Synonyms:phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

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Chemical Property of phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

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Technology Process of phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

There total 5 articles about phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 288089-41-8
Phosphoric acid bis-((S)-2,3-dihydroxy-propyl) ester 2-(methyl-diphenyl-silanyl)-ethyl ester

: 288089-42-9
phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 4 ℃; for 16h;

Reference yield:

: 40438-48-0
diphenylmethylsilylethylethanol

: 288089-42-9
phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: PCl₃ / CH₂Cl₂; diethyl ether; diethyl ether / 3 h / 20 °C

2: pyridine / CH₂Cl₂; diethyl ether; diethyl ether / 1 h / 20 °C

3: 274 mg / mCPBA; pyridine / CH₂Cl₂; diethyl ether; diethyl ether / 0.5 h / 20 °C

4: 84 percent / AcOH / H₂O / 0.75 h / 60 °C

5: 82 percent / imidazole / dimethylformamide / 16 h / 4 °C

With pyridine; 1H-imidazole; acetic acid; 3-chloro-benzenecarboperoxoic acid; phosphorus trichloride; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 1: Substitution / 2: Condensation / 3: Oxidation / 4: Hydrolysis / 5: Substitution;

Reference yield:

: 289698-26-6
C₁₅H₁₇Cl₂OPSi

: 288089-42-9
phosphoric acid bis-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl] ester 2-(methyl-diphenyl-silanyl)-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / CH₂Cl₂; diethyl ether; diethyl ether / 1 h / 20 °C

2: 274 mg / mCPBA; pyridine / CH₂Cl₂; diethyl ether; diethyl ether / 0.5 h / 20 °C

3: 84 percent / AcOH / H₂O / 0.75 h / 60 °C

4: 82 percent / imidazole / dimethylformamide / 16 h / 4 °C

With pyridine; 1H-imidazole; acetic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 1: Condensation / 2: Oxidation / 3: Hydrolysis / 4: Substitution;