1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene

Base Information

Chemical Name:1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene
CAS No.:444727-37-1
Molecular Formula:C₃₆H₄₆O₅S
Molecular Weight:590.824
Hs Code.:

Synonyms:1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene

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Chemical Property of 1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene

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Technology Process of 1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene

There total 14 articles about 1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 127441-50-3
4-(2-(2-hydroxyethoxy)ethoxy)benzaldehyde

: 444727-34-8
{{4-{2-[4-(decylsulfonyl)phenyl]ethenyl}phenyl}methyl}phosphonic acid diethyl ester

: 444727-37-1
1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 2h;
DOI:10.1016/S0040-4020(02)00003-0

Reference yield:

: 127441-50-3
4-(2-(2-hydroxyethoxy)ethoxy)benzaldehyde

: diethyl 4-(4-decylsulfonylstyryl)benzylphosphonate

: 444727-37-1
1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene

Guidance literature:: With sodium hydride; In 1,2-dimethoxyethane; at 0 - 20 ℃; for 2.5h;
DOI:10.1039/a803229g

Reference yield:

: 157376-04-0
4-(decylthio)benzaldehyde

: 444727-37-1
1-<4-<2-(2-hydroxyethoxy)ethoxy>styryl>-4-(4-decylsulfonylstyryl)benzene

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / NaH / tetrahydrofuran / 1 h / 0 - 20 °C

2: 98 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

3: 70 percent / Ph₃PBr₂ / CH₂Cl₂ / 2 h / Heating

4: 97 percent / 2 h / Heating

5: 98 percent / MCPBA / CH₂Cl₂ / 2 h / 0 °C

6: 78 percent / NaH / tetrahydrofuran / 2 h / 0 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; triphenylphosphine dibromide 1:1 addition complex; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; 6: Wittig-Horner reaction;
DOI:10.1016/S0040-4020(02)00003-0