1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate

Base Information

Chemical Name:1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate
CAS No.:1005789-21-8
Molecular Formula:C₁₈H₁₉BrN₃*ClO₄
Molecular Weight:456.724
Hs Code.:

Synonyms:1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate

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Chemical Property of 1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate

Chemical Property:

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Technology Process of 1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate

There total 4 articles about 1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-40-1
4-bromo-aniline

: 1005789-21-8
1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / 1,2-dichloro-benzene / 12 h / 190 °C

2.1: sodium iodide / acetic acid / 1.5 h

2.2: 10 h

With trifluoroacetic acid; sodium iodide; In acetic acid; 1,2-dichloro-benzene;
DOI:10.1039/c4dt01353k

Reference yield:

: 825-56-9
2-phenyl-1,3,4-oxadiazole

: 1005789-21-8
1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / 1,2-dichloro-benzene / 12 h / 190 °C

2.1: sodium iodide / acetic acid / 1.5 h

2.2: 10 h

With trifluoroacetic acid; sodium iodide; In acetic acid; 1,2-dichloro-benzene;
DOI:10.1039/c4dt01353k

Reference yield:

: 507-20-0
tertiary butyl chloride

: 575444-93-8
4-(4-bromophenyl)-3-phenyl-4H-1,2,4-triazole

: 1005789-21-8
1-tert-butyl-3-phenyl-4-(4-bromophenyl)-1,2,4-triazolium perchlorate

Guidance literature:: tertiary butyl chloride; With sodium iodide; In acetic acid; for 1.5h;

4-(4-bromophenyl)-3-phenyl-4H-1,2,4-triazole; In acetic acid; for 10h;

With sodium perchlorate; sodium sulfite; In water; acetic acid;
DOI:10.1039/c4dt01353k