2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Base Information

Chemical Name:2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate
CAS No.:1427435-27-5
Molecular Formula:C₃₇H₆₄O₈Si₃
Molecular Weight:721.167
Hs Code.:

Synonyms:2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

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Chemical Property of 2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

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Technology Process of 2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

There total 9 articles about 2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427435-25-3
3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoic acid

: 1427435-26-4
2,3-bis(tert-butyldimethylsilyl ether)benzyl alcohol

: 1427435-27-5
2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 1427435-27-5
2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: sodium tetrahydroborate / isopropyl alcohol / 0 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

With dmap; sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 1427435-24-2
methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

: 1427435-27-5
2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / methanol; water / 60 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In methanol; dichloromethane; water;