methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Base Information

Chemical Name:methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate
CAS No.:1427435-24-2
Molecular Formula:C₁₉H₃₂O₆Si
Molecular Weight:384.545
Hs Code.:

Synonyms:methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Chemical Property:

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Technology Process of methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

There total 4 articles about methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 1427435-23-1
methyl 3-(tert-butyldimethylsilyloxymethyl)-4-hydroxybenzoate

: 1427435-24-2
methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 1427435-22-0
methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(tert-butyldimethylsilyloxy)benzoate

: 1427435-24-2
methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / methanol; water / 0 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; dichloromethane; water;

Reference yield:

: 59648-31-6
4-hydroxy-3-hydroxymethylbenzoic acid methyl ester

: 1427435-24-2
methyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: lithium hydroxide / methanol; water / 0 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;