2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate

Base Information

Chemical Name:2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate
CAS No.:1427435-28-6
Molecular Formula:C₂₇H₄₂O₆Si₂
Molecular Weight:518.798
Hs Code.:

Synonyms:2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate

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Chemical Property of 2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate

Chemical Property:

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Technology Process of 2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate

There total 11 articles about 2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427435-27-5
2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(tert-butyldimethylsilyloxymethyl)-4-(2-methoxyethoxymethyl)oxybenzoate

: 1427435-28-6
2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate

Guidance literature:: With pyridinium p-toluenesulfonate; In isopropyl alcohol; at 80 ℃;

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 1427435-28-6
2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: sodium tetrahydroborate / isopropyl alcohol / 0 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

4: pyridinium p-toluenesulfonate / isopropyl alcohol / 80 °C

With dmap; sodium tetrahydroborate; pyridinium p-toluenesulfonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 1427435-26-4
2,3-bis(tert-butyldimethylsilyl ether)benzyl alcohol

: 1427435-28-6
2,3-di(tert-butyldimethylsilyloxy)benzyl 3-(hydroxymethyl)-4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

2: pyridinium p-toluenesulfonate / isopropyl alcohol / 80 °C

With dmap; pyridinium p-toluenesulfonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; isopropyl alcohol;