C₂₅H₂₀ClF₃N₆O₆S

Base Information

Chemical Name:C₂₅H₂₀ClF₃N₆O₆S
CAS No.:1612242-74-6
Molecular Formula:C₂₅H₂₀ClF₃N₆O₆S
Molecular Weight:624.985
Hs Code.:

C<sub>25</sub>H<sub>20</sub>ClF<sub>3</sub>N<sub>6</sub>O<sub>6</sub>S

Synonyms:C₂₅H₂₀ClF₃N₆O₆S

Suppliers and Price of C₂₅H₂₀ClF₃N₆O₆S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₂₀ClF₃N₆O₆S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₂₀ClF₃N₆O₆S

There total 9 articles about C₂₅H₂₀ClF₃N₆O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1612243-46-5
N-[(S)-2-amino-2-(4-chloro-3-trifluoromethyl-phenyl)-ethyl]-N-methyl-4-nitro-benzenesulfonamide

: methyl 4-hydroxypyrido[3,2-d]pyrimidine-8-carboxylate

: 1612242-74-6
C₂₅H₂₀ClF₃N₆O₆S

Guidance literature:: methyl 4-hydroxypyrido[3,2-d]pyrimidine-8-carboxylate; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 ℃; for 0.166667h; Inert atmosphere;

N-[(S)-2-amino-2-(4-chloro-3-trifluoromethyl-phenyl)-ethyl]-N-methyl-4-nitro-benzenesulfonamide; In dimethyl sulfoxide; at 40 ℃;

Reference yield:

: 6635-86-5,67476-70-4
2-amino-4-methyl-3-nitropyridine

: 1612242-74-6
C₂₅H₂₀ClF₃N₆O₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium nitrite; sulfuric acid / water / 2 h / 0 - 20 °C

2.1: phosphorus(V) oxybromide / 1,2-dichloro-ethane / 12 h / 20 °C / Reflux

3.1: N,N-dimethyl-formamide / 13 h / 100 °C

4.1: sulfuric acid / water / 3 h / 70 °C

5.1: hydrogenchloride; ammonium chloride; iron / water; isopropyl alcohol / Reflux

6.1: 24 h / Reflux

7.1: sulfuric acid; potassium dichromate; Pyrimidin-2(1H)-one / water / 20 - 30 °C

8.1: 1,1'-carbonyldiimidazole / 1-methyl-pyrrolidin-2-one / 70 °C

8.2: 70 °C

9.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

9.2: 40 °C

With Pyrimidin-2(1H)-one; hydrogenchloride; potassium dichromate; sulfuric acid; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; sodium nitrite; phosphorus(V) oxybromide; In 1-methyl-pyrrolidin-2-one; water; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 21901-18-8
4-Methyl-3-nitro-2-pyridone

: 1612242-74-6
C₂₅H₂₀ClF₃N₆O₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: phosphorus(V) oxybromide / 1,2-dichloro-ethane / 12 h / 20 °C / Reflux

2.1: N,N-dimethyl-formamide / 13 h / 100 °C

3.1: sulfuric acid / water / 3 h / 70 °C

4.1: hydrogenchloride; ammonium chloride; iron / water; isopropyl alcohol / Reflux

5.1: 24 h / Reflux

6.1: sulfuric acid; potassium dichromate; Pyrimidin-2(1H)-one / water / 20 - 30 °C

7.1: 1,1'-carbonyldiimidazole / 1-methyl-pyrrolidin-2-one / 70 °C

7.2: 70 °C

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

8.2: 40 °C

With Pyrimidin-2(1H)-one; hydrogenchloride; potassium dichromate; sulfuric acid; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; phosphorus(V) oxybromide; In 1-methyl-pyrrolidin-2-one; water; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; isopropyl alcohol;