Technology Process of C35H41NO10
There total 5 articles about C35H41NO10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
DOI:10.1039/c2ob26928g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 5 h / -10 °C / Molecular sieve; Inert atmosphere
2: trifluoroacetic acid / dichloromethane; methanol / 0.5 h / 0 °C
3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 6 h / 0 °C
4: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C
With
N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifluorormethanesulfonic acid; [bis(acetoxy)iodo]benzene; potassium carbonate; trifluoroacetic acid;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26928g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / dichloromethane; methanol / 0.5 h / 0 °C
2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 6 h / 0 °C
3: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; potassium carbonate; trifluoroacetic acid;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26928g