C₃₇H₃₈BrNO₇

Base Information

Chemical Name:C₃₇H₃₈BrNO₇
CAS No.:1384190-48-0
Molecular Formula:C₃₇H₃₈BrNO₇
Molecular Weight:688.615
Hs Code.:

C<sub>37</sub>H<sub>38</sub>BrNO<sub>7</sub>

Synonyms:C₃₇H₃₈BrNO₇

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Chemical Property of C₃₇H₃₈BrNO₇

Chemical Property:

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Technology Process of C₃₇H₃₈BrNO₇

There total 13 articles about C₃₇H₃₈BrNO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 125416-37-7
(R)-mandelic acid piperidine amide

: 1206902-68-2
2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

: 1384190-48-0
C₃₇H₃₈BrNO₇

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -20 ℃; for 14h;
DOI:10.1055/s-0031-1290658

Reference yield:

: 1384190-36-6
2-allyl-4-bromo-6-methoxyphenol 3'-methoxy-4'-benzyloxybenzyl ether

: 1384190-48-0
C₃₇H₃₈BrNO₇

Guidance literature:: Multi-step reaction with 4 steps

1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 4 h / 0 - 20 °C

2: lead(IV) tetraacetate; potassium carbonate / benzene / 3 h / 0 - 20 °C

3: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 0 °C

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 14 h / -20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; lead(IV) tetraacetate; potassium carbonate; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol; benzene;
DOI:10.1055/s-0031-1290658

Reference yield:

: 90-05-1
2-methoxy-phenol

: 1384190-48-0
C₃₇H₃₈BrNO₇

Guidance literature:: Multi-step reaction with 8 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 1 h / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

3: N,N-diethylaniline / 20 h / 20 - 190 °C

4: potassium carbonate / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

5: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 4 h / 0 - 20 °C

6: lead(IV) tetraacetate; potassium carbonate / benzene / 3 h / 0 - 20 °C

7: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 0 °C

8: dmap; dicyclohexyl-carbodiimide / dichloromethane / 14 h / -20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; N-Bromosuccinimide; osmium(VIII) oxide; 2-methyl-but-2-ene; lead(IV) tetraacetate; potassium carbonate; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; N,N-diethylaniline; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol; benzene; 3: Claisen rearrangement;
DOI:10.1055/s-0031-1290658