(8R,8'R)-(-)-thujaplicatin methyl ether

Base Information

Chemical Name:(8R,8'R)-(-)-thujaplicatin methyl ether
CAS No.:228556-52-3
Molecular Formula:C₂₁H₂₄O₇
Molecular Weight:388.417
Hs Code.:

Synonyms:(8R,8'R)-(-)-thujaplicatin methyl ether

Suppliers and Price of (8R,8'R)-(-)-thujaplicatin methyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (8R,8'R)-(-)-thujaplicatin methyl ether

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of (8R,8'R)-(-)-thujaplicatin methyl ether

There total 8 articles about (8R,8'R)-(-)-thujaplicatin methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 111194-06-0
(-)-O-dibenzylthujaplicatin methyl ether

: 228556-52-3,6512-67-0
(8R,8'R)-(-)-thujaplicatin methyl ether

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 15h; under 2250.2 Torr;
DOI:10.3987/R-1987-05-1169

Reference yield:

: 2176-18-3
4-benzyloxy-3,5-dimethoxybenzyl alcohol

: 228556-52-3,6512-67-0
(8R,8'R)-(-)-thujaplicatin methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / PBr₃ / diethyl ether

2: 1.) LDA / 1.) THF, 2.) THF, -80 deg C, 3 h

3: 78 percent / H₂ / Pd/C / ethyl acetate / 15 h / 2250.2 Torr

With hydrogen; phosphorus tribromide; lithium diisopropyl amide; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.3987/R-1987-05-1169

Reference yield:

: 6527-32-8
4-(benzyloxy)-3,5-dimethoxybenzaldehyde

: 228556-52-3,6512-67-0
(8R,8'R)-(-)-thujaplicatin methyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / NaBH₄

2: 100 percent / PBr₃ / diethyl ether

3: 1.) LDA / 1.) THF, 2.) THF, -80 deg C, 3 h

4: 78 percent / H₂ / Pd/C / ethyl acetate / 15 h / 2250.2 Torr

With sodium tetrahydroborate; hydrogen; phosphorus tribromide; lithium diisopropyl amide; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.3987/R-1987-05-1169