(E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate

Base Information

Chemical Name:(E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate
CAS No.:1370723-34-4
Molecular Formula:C₁₈H₂₅BO₅
Molecular Weight:332.204
Hs Code.:

Synonyms:(E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate

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Chemical Property of (E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate

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Technology Process of (E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate

There total 3 articles about (E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 167896-49-3
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-ol

: 541-41-3
chloroformic acid ethyl ester

: 1370723-34-4
(E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate

Guidance literature:: With pyridine; dmap; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201100806

Reference yield:

: 1138162-59-0
C₁₈H₂₉BO₃Si

: 1370723-34-4
(E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water / 0 - 20 °C

2: pyridine; dmap / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; In tetrahydrofuran; water;
DOI:10.1002/adsc.201100806

Reference yield:

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1370723-34-4
(E)-ethyl [1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl] carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 48 h / 100 °C / Sealed tube; Inert atmosphere

2: hydrogenchloride / tetrahydrofuran; water / 0 - 20 °C

3: pyridine; dmap / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; In tetrahydrofuran; water;
DOI:10.1002/adsc.201100806