9,10-diphenyl-9,10-dihydro-10-germa-9-sila-9,10[1'2']benzenoanthracene

Base Information

• Chemical Name: 9,10-diphenyl-9,10-dihydro-10-germa-9-sila-9,10[1'2']benzenoanthracene
• CAS No.: 263772-61-8
• Molecular Formula: C₃₀H₂₂GeSi
• Molecular Weight: 483.18
• Mol file: 263772-61-8.mol

Synonyms:9,10-diphenyl-9,10-dihydro-10-germa-9-sila-9,10[1'2']benzenoanthracene

Chemical Property of 9,10-diphenyl-9,10-dihydro-10-germa-9-sila-9,10[1'2']benzenoanthracene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,10-diphenyl-9,10-dihydro-10-germa-9-sila-9,10[1'2']benzenoanthracene

There total 1 articles about 9,10-diphenyl-9,10-dihydro-10-germa-9-sila-9,10[1'2']benzenoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

10-phenyl-9,10-dihydro-10-germa-9-sila-9,10[1',2']-benzenoanthracene (204135-21-7) + phenyllithium (591-51-5) → 9,10-diphenyl-9,10-dihydro-10-germa-9-sila-9,10[1'2']benzenoanthracene (263772-61-8)

Guidance literature:

With NH₄Cl; In diethyl ether; cyclohexane; under argon, Schlenk setup, 1:6 mixt., after 1 min satd. NH4Cl soln. added; extd. (CHCl3), filtered, dried (MgSO4), evapd., washed (Et2O), elem. anal.;

DOI:10.1021/om990976o

upstream raw materials:

10-phenyl-9,10-dihydro-10-germa-9-sila-9,10[1',2']-benzenoanthracene

phenyllithium