C₂₃H₂₇BrN₂O₂Si

Base Information

Chemical Name:C₂₃H₂₇BrN₂O₂Si
CAS No.:1379526-10-9
Molecular Formula:C₂₃H₂₇BrN₂O₂Si
Molecular Weight:471.469
Hs Code.:

C<sub>23</sub>H<sub>27</sub>BrN<sub>2</sub>O<sub>2</sub>Si

Synonyms:C₂₃H₂₇BrN₂O₂Si

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Chemical Property of C₂₃H₂₇BrN₂O₂Si

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Technology Process of C₂₃H₂₇BrN₂O₂Si

There total 4 articles about C₂₃H₂₇BrN₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19158-51-1
P-toluenesulfonyl cyanide

: 1379526-09-6
C₂₂H₂₈BrNO₂Si

: 1379526-10-9
C₂₃H₂₇BrN₂O₂Si

Guidance literature:: C₂₂H₂₈BrNO₂Si; With lithium hexamethyldisilazane; In toluene; at -78 - 0 ℃; for 0.25h; Inert atmosphere;

P-toluenesulfonyl cyanide; In toluene; at -78 ℃; for 0.0333333h; Inert atmosphere;

With water; In toluene; at -78 - 24 ℃; for 0.5h; pH=7; Sodium phosphate buffer; Inert atmosphere;

Reference yield:

: 3839-31-4
dimethyl(phenyl)silyl lithium

: 1379526-10-9
C₂₃H₂₇BrN₂O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

1.2: 3.08 h / -78 - -23 °C / Inert atmosphere

1.3: 1.5 h / -78 - -23 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / toluene / 0.25 h / -78 - 0 °C / Inert atmosphere

2.2: 0.03 h / -78 °C / Inert atmosphere

2.3: 0.5 h / -78 - 24 °C / pH 7 / Sodium phosphate buffer; Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;

Reference yield:

: 156094-64-3
2-(bromomethyl)-3-bromo-6-methoxypyridine

: 1379526-10-9
C₂₃H₂₇BrN₂O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

1.2: 3.08 h / -78 - -23 °C / Inert atmosphere

1.3: 1.5 h / -78 - -23 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / toluene / 0.25 h / -78 - 0 °C / Inert atmosphere

2.2: 0.03 h / -78 °C / Inert atmosphere

2.3: 0.5 h / -78 - 24 °C / pH 7 / Sodium phosphate buffer; Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;