(S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate

Base Information

Chemical Name:(S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate
CAS No.:1012325-69-7
Molecular Formula:C₃₇H₆₆O₈Si₃
Molecular Weight:723.183
Hs Code.:

Synonyms:(S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate

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Chemical Property of (S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate

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Technology Process of (S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate

There total 1 articles about (S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 1012325-62-0
C₃₄H₅₈O₈Si₂

: 1012325-69-7
(S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate

Guidance literature:: C₃₄H₅₈O₈Si₂; With lithium diisopropyl amide; In tetrahydrofuran; at -78 - -20 ℃; for 0.5h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol702961v

Reference yield:

: 1012325-69-7
(S)-5-(trimethylsilyl)pent-4-yn-2-yl 2-((S,E)-5,6-bis(tert-butyldimethylsilyloxy)hex-1-enyl)-4,6-bis(methoxymethoxy)benzoate

: C₃₁H₅₂O₈Si₂

Guidance literature:: With pyridine hydrofluoride; In tetrahydrofuran; at -20 - 0 ℃; for 38h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol702961v