Technology Process of C19H15ClF6N4O4*ClH
There total 6 articles about C19H15ClF6N4O4*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane;
at 20 ℃;
for 2h;
DOI:10.1021/jm3007596
- Guidance literature:
-
Multi-step reaction with 5 steps
1: phosphorus trichloride / 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane / 2 h
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran; dichloromethane / 14 h / 20 °C
3: trifluoroacetic acid / dichloromethane
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C
5: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
With
hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; phosphorus trichloride;
In
tetrahydrofuran; 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1021/jm3007596
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran; dichloromethane / 14 h / 20 °C
2: trifluoroacetic acid / dichloromethane
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C
4: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
With
hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/jm3007596
