Technology Process of C16H22O2
There total 8 articles about C16H22O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H20O;
With
C20H25N3O; dihydrogen peroxide; trichloroacetic acid;
In
1,4-dioxane; water;
at 32 ℃;
for 48h;
With
triethyl phosphite;
In
1,4-dioxane; water;
at 32 ℃;
for 21h;
optical yield given as %ee;
DOI:10.1039/c0cc02332a
- Guidance literature:
-
With
D-Prolin;
In
isopropyl alcohol;
at 20 ℃;
for 72h;
optical yield given as %ee;
DOI:10.1039/c0cc02332a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium periodate / tetrahydrofuran; water / 7.5 h / 20 °C
2.1: D-Prolin / isopropyl alcohol / 72 h / 20 °C
3.1: C20H25N3O; dihydrogen peroxide; trichloroacetic acid / 1,4-dioxane; water / 48 h / 32 °C
3.2: 21 h / 32 °C
With
sodium periodate; C20H25N3O; dihydrogen peroxide; D-Prolin; trichloroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; water; isopropyl alcohol;
2.1: Aldol condensation / 3.1: oxa-Michael addition;
DOI:10.1039/c0cc02332a