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Technology Process of (C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]

(C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]

Base Information
  • Chemical Name:(C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]
  • CAS No.:1020853-38-6
  • Molecular Formula:C16H36N*C37H65Ga2SSi
  • Molecular Weight:951.989
  • Hs Code.:
(C<sub>4</sub>H<sub>9</sub>)4N<sup>(1+)</sup>*[C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]<sup>(1-)</sup>=[(C<sub>4</sub>H<sub>9</sub>)4N][C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]

Synonyms:(C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]

Suppliers and Price of (C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]
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Chemical Property of (C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]
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Technology Process of (C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]

There total 3 articles about (C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2
1020853-36-4

C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2

tetra-N-butylammonium benzenethiolate
4670-62-6

tetra-N-butylammonium benzenethiolate

(C<sub>4</sub>H<sub>9</sub>)4N<sup>(1+)</sup>*[C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]<sup>(1-)</sup>=[(C<sub>4</sub>H<sub>9</sub>)4N][C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]
1020853-38-6

(C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]

Guidance literature:
In further solvent(s); (Ar); mixt. of thiophenolate in 1,2-difluorobenzene was added dropwise to Ga compd. in 1,2-difluorobenzene at room temp.; stirred for 3 h; concd.; cooled to 4°C; elem. anal.;
DOI:10.1021/om800068s

Reference yield:

neopentyl lithium
7412-67-1

neopentyl lithium

(C<sub>4</sub>H<sub>9</sub>)4N<sup>(1+)</sup>*[C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]<sup>(1-)</sup>=[(C<sub>4</sub>H<sub>9</sub>)4N][C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]
1020853-38-6

(C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]

Guidance literature:
Multi-step reaction with 2 steps
1: toluene
2: further solvent(s)
In toluene;
DOI:10.1021/om800068s

Reference yield:

[C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(GaCl<sub>2</sub>)2]2
1005391-33-2

[C6H5CH2C(Si(CH3)3)(GaCl2)2]2

(C<sub>4</sub>H<sub>9</sub>)4N<sup>(1+)</sup>*[C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]<sup>(1-)</sup>=[(C<sub>4</sub>H<sub>9</sub>)4N][C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2SC<sub>6</sub>H<sub>5</sub>]
1020853-38-6

(C4H9)4N(1+)*[C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5](1-)=[(C4H9)4N][C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2SC6H5]

Guidance literature:
Multi-step reaction with 2 steps
1: toluene
2: further solvent(s)
In toluene;
DOI:10.1021/om800068s
upstream raw materials:

C6H5CH2C(Si(CH3)3)(Ga(CH2C(CH3)3)2)2

tetra-N-butylammonium benzenethiolate

[C6H5CH2C(Si(CH3)3)(GaCl2)2]2

neopentyl lithium

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