2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

Base Information

Chemical Name:2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide
CAS No.:1207315-60-3
Molecular Formula:C₁₆H₆ClF₇I₂N₂O₃
Molecular Weight:696.486
Hs Code.:

Synonyms:2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

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Chemical Property of 2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

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Technology Process of 2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

There total 4 articles about 2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1152247-48-7
2,6-diiodo-4-heptafluoroisopropylaniline

: 34128-16-0
2-chloro-3-nitro-benzoyl chloride

: 1207315-60-3
2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

Guidance literature:: With 1,3-dimethyl-2-imidazolidinone; at 135 ℃; for 3h;

Reference yield:

: 3970-35-2
2-chloro-3-nitrobezoic acid

: 1207315-60-3
2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / tetrahydrofuran

2: 1,3-dimethyl-2-imidazolidinone / 3 h / 135 °C

With 1,3-dimethyl-2-imidazolidinone; thionyl chloride; In tetrahydrofuran;

Reference yield:

: 62-53-3
aniline

: 1207315-60-3
2-chloro-N-(2,6-diiodo-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium dithionite / ethyl acetate; water / 6 h / 20 °C

2: sulfuric acid; N-iodo-succinimide / ethanol / 3 h / 5 - 20 °C

3: 1,3-dimethyl-2-imidazolidinone / 3 h / 135 °C

With 1,3-dimethyl-2-imidazolidinone; N-iodo-succinimide; sodium dithionite; sulfuric acid; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; In ethanol; water; ethyl acetate;