Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester

Base Information

Chemical Name:Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester
CAS No.:81121-46-2
Molecular Formula:C₁₇H₂₆O₃
Molecular Weight:278.392
Hs Code.:

Synonyms:Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester

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Chemical Property of Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester

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Technology Process of Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester

There total 7 articles about Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65519-73-5
6-isopropoxymethylene-2,2-dimethyl-cyclohexanone

: 81121-46-2
Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-butyllithium / 1.) THF, hexane, -65 - 0 deg C, 2.) -65 deg C up to room temp., 1 h

2: 1 N H₂SO₄ / acetone / 0.5 h

3: LiAlH₄ / diethyl ether / 3 h / Ambient temperature

4: pyridine / diethyl ether / 2 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; In diethyl ether; acetone;
DOI:10.1021/jo00348a043

Reference yield:

: 76337-17-2
2-formyl-6,6-dimethylcyclohexanone

: 81121-46-2
Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / potassium carbonate / acetone / 6 h / Heating

2: 1.) n-butyllithium / 1.) THF, hexane, -65 - 0 deg C, 2.) -65 deg C up to room temp., 1 h

3: 1 N H₂SO₄ / acetone / 0.5 h

4: LiAlH₄ / diethyl ether / 3 h / Ambient temperature

5: pyridine / diethyl ether / 2 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; potassium carbonate; In diethyl ether; acetone;
DOI:10.1021/jo00348a043

Reference yield:

: 81121-44-0
rac-5-(6,6-dimethyl-2-formyl-1-cyclohexen-1-yl)-3-methyl-3-hydroxy-1-penten-4-yne

: 81121-46-2
Acetic acid 2-((E)-3-hydroxy-3-methyl-penta-1,4-dienyl)-3,3-dimethyl-cyclohex-1-enylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 3 h / Ambient temperature

2: pyridine / diethyl ether / 2 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jo00348a043