Cyclohexanone, 2,2-dimethyl-6-[(1-methylethoxy)methylene]-

Base Information

Chemical Name:Cyclohexanone, 2,2-dimethyl-6-[(1-methylethoxy)methylene]-
CAS No.:65519-73-5
Molecular Formula:C12H20O2
Molecular Weight:196.28600
Hs Code.:

Synonyms:Cyclohexanone,2,2-dimethyl-6-[(1-methylethoxy)methylene];6-Isopropoxymethylen-2,2-dimethyl-cyclohexanon;6-isopropoxymethylene-2,2-dimethyl-cyclohexanone;6-Isopropyloxymethylen-2,2-dimethyl-cyclohexanon;

Suppliers and Price of Cyclohexanone, 2,2-dimethyl-6-[(1-methylethoxy)methylene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Cyclohexanone, 2,2-dimethyl-6-[(1-methylethoxy)methylene]-

Chemical Property:

PSA：26.30000
LogP:3.07450

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanone, 2,2-dimethyl-6-[(1-methylethoxy)methylene]-

There total 7 articles about Cyclohexanone, 2,2-dimethyl-6-[(1-methylethoxy)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75-30-9
2-iodo-propane

: 76337-17-2
2-formyl-6,6-dimethylcyclohexanone

: 65519-73-5
6-isopropoxymethylene-2,2-dimethyl-cyclohexanone

Guidance literature:: With potassium carbonate; In acetone; for 6h; Heating;
DOI:10.1021/jo00348a043

Reference yield:

: 65519-68-8
2-(isopropoxymethylene)-6-methylcyclohexanone

: 865-47-4
potassium tert-butylate

: 74-88-4
methyl iodide

: 1352237-61-6
(E)-6-(tert-butoxymethylene)-2,2-dimethylcyclohexanone

: 65519-73-5
(E)-6-(isopropoxymethylene)-2,2-dimethylcyclohexanone

Guidance literature:: 2-(isopropoxymethylene)-6-methylcyclohexanone; potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.166667h;

methyl iodide; In tetrahydrofuran; at 20 ℃; Overall yield = 3.52 g; Reflux;

Reference yield:

: 75-30-9
2-iodo-propane

: 65519-73-5
6-isopropoxymethylene-2,2-dimethyl-cyclohexanone

Guidance literature:: With potassium carbonate; acetone; und Behandeln des vorwiegend aus 3-Methyl-1-isopropyloxymethylen-cyclohexanon-⁽²⁾ bestehenden Reaktionsprodukts mit Kalium-tert-butylat in tert-Butylalkohol bei 0grad und anschliessend mit Methyljodid;
DOI:10.1021/ja01198a036 DOI:10.1002/hlca.19510340236