(E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol

Base Information

Chemical Name:(E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol
CAS No.:81121-45-1
Molecular Formula:C₁₅H₂₄O₂
Molecular Weight:236.354
Hs Code.:

Synonyms:(E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol

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Chemical Property of (E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol

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Technology Process of (E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol

There total 6 articles about (E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81121-44-0
rac-5-(6,6-dimethyl-2-formyl-1-cyclohexen-1-yl)-3-methyl-3-hydroxy-1-penten-4-yne

: 81121-45-1
(E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 3h; Ambient temperature;
DOI:10.1021/jo00348a043

Reference yield:

: 65519-73-5
6-isopropoxymethylene-2,2-dimethyl-cyclohexanone

: 81121-45-1
(E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium / 1.) THF, hexane, -65 - 0 deg C, 2.) -65 deg C up to room temp., 1 h

2: 1 N H₂SO₄ / acetone / 0.5 h

3: LiAlH₄ / diethyl ether / 3 h / Ambient temperature

With lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; In diethyl ether; acetone;
DOI:10.1021/jo00348a043

Reference yield:

: 76337-17-2
2-formyl-6,6-dimethylcyclohexanone

: 81121-45-1
(E)-1-(2-Hydroxymethyl-6,6-dimethyl-cyclohex-1-enyl)-3-methyl-penta-1,4-dien-3-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / potassium carbonate / acetone / 6 h / Heating

2: 1.) n-butyllithium / 1.) THF, hexane, -65 - 0 deg C, 2.) -65 deg C up to room temp., 1 h

3: 1 N H₂SO₄ / acetone / 0.5 h

4: LiAlH₄ / diethyl ether / 3 h / Ambient temperature

With lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; potassium carbonate; In diethyl ether; acetone;
DOI:10.1021/jo00348a043