(1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

Base Information

Chemical Name:(1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane
CAS No.:355410-72-9
Molecular Formula:C₁₉H₁₉NO₃
Molecular Weight:309.365
Hs Code.:

Synonyms:(1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

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Chemical Property of (1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

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Technology Process of (1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

There total 2 articles about (1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 100-52-7
benzaldehyde

: 54623-66-4
(4S,5S)-(-)-2-chloromethyl-4-methoxymethyl-5-phenyl-2-oxazoline

: 355410-72-9
(1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

Guidance literature:: (4S,5S)-(-)-2-chloromethyl-4-methoxymethyl-5-phenyl-2-oxazoline; With titanium(IV) isopropylate; lithium diisopropyl amide; In tetrahydrofuran; at -98 ℃; for 0.266667h;

benzaldehyde; In tetrahydrofuran; at -98 - 20 ℃;

With sodium hydroxide; In isopropyl alcohol;
DOI:10.1002/1099-0690(200106)2001:11<2035::AID-EJOC2035>3.0.CO;2-R

Reference yield:

: 1028306-32-2
2-Chloro-2-((4S,5S)-4-methoxymethyl-5-phenyl-4,5-dihydro-oxazol-2-yl)-1-phenyl-ethanol

: (1S,2S,4'S,5'S)-cis-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

: 355410-72-9
(1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

: (1R,2S,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

: (1R,2R,4'S,5'S)-cis-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

Guidance literature:: With sodium hydroxide; water; In isopropyl alcohol; Further Variations:; Reagents; Product distribution;
DOI:10.1002/1099-0690(200106)2001:11<2035::AID-EJOC2035>3.0.CO;2-R

Reference yield:

: 355410-72-9
(1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane

: 121651-02-3
(2S,3R)-2-formyl-3-phenyloxirane

Guidance literature:: (1S,2R,4'S,5'S)-trans-1,2-epoxy-1-(4-methoxymethyl-5-phenyl-2-oxazolin-2-yl)-2-phenylethane; With methyl trifluoromethanesulfonate;

With sodium tetrahydroborate;

With oxalic acid;
DOI:10.1002/1099-0690(200106)2001:11<2035::AID-EJOC2035>3.0.CO;2-R