methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate

Base Information

Chemical Name:methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate
CAS No.:1365721-06-7
Molecular Formula:C₂₂H₂₃N₅O₄S₂
Molecular Weight:485.588
Hs Code.:

Synonyms:methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate

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Chemical Property of methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate

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Technology Process of methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate

There total 9 articles about methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 67-56-1
methanol

: 1365718-87-1
[5-(3-{[(5-isopropyl-3-methyl-1-benzothien-2-yl)sulfonyl]amino}phenyl)-2H-tetrazol-2-yl]acetic acid

: 1365721-06-7
methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate

Guidance literature:: With pyridine; 1,1'-carbonyldiimidazole; In acetonitrile; at 20 ℃;

Reference yield:

: 1353433-18-7
5-isopropyl-3-methylbenzothiophene-2-sulfonic acid

: 1365721-06-7
methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus pentachloride; trichlorophosphate / dichloromethane / 2 h / 20 °C

2: pyridine / dichloromethane / 2 h / 20 °C

3: sodium hydroxide; water / 0.08 h / 20 °C

4: pyridine; 1,1'-carbonyldiimidazole / acetonitrile / 20 °C

With pyridine; phosphorus pentachloride; water; 1,1'-carbonyldiimidazole; sodium hydroxide; trichlorophosphate; In dichloromethane; acetonitrile;

Reference yield:

: 1365722-03-7
C₂₃H₂₅N₅O₄S₂

: 1365721-06-7
methyl {5-[3-({[3-methyl-5-(1-methylethyl)-1-benzothiophen-2-yl]sulfonyl}amino)phenyl]-2H-tetrazol-2-yl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / 0.08 h / 20 °C

2: pyridine; 1,1'-carbonyldiimidazole / acetonitrile / 20 °C

With pyridine; water; 1,1'-carbonyldiimidazole; sodium hydroxide; In acetonitrile;