4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide
CAS No.:947527-46-0
Molecular Formula:C₁₈H₂₃NO₂S
Molecular Weight:317.452
Hs Code.:

Synonyms:4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide

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Chemical Property of 4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide

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Technology Process of 4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide

There total 3 articles about 4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6153-05-5,105-29-3
(Z)-3-methylpent-2-en-4-ynol

: 78388-19-9
4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

: 947527-46-0
4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide

Guidance literature:: (Z)-3-methylpent-2-en-4-ynol; With n-butyllithium; methanesulfonyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.666667h; Inert atmosphere;

With lithium bromide; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 1h; Inert atmosphere;

4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide; With sodium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201805908

Reference yield:

: 85850-08-4
(Z)-1-bromo-3-methylpent-2-en-4-yne

: 947527-46-0
4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃ / acetone / Heating

2: 76 percent / K₂CO₃ / acetone / Heating

With potassium carbonate; In acetone;
DOI:10.1021/ol0713032

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 947527-46-0
4-methyl-N-(3-methyl-but-2-enyl)-N-((Z)-3-methyl-pent-2-en-4-ynyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃ / acetone / Heating

2: 76 percent / K₂CO₃ / acetone / Heating

With potassium carbonate; In acetone;
DOI:10.1021/ol0713032