(2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid

Base Information

Chemical Name:(2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid
CAS No.:1623063-20-6
Molecular Formula:C₂₅H₃₇NO₈
Molecular Weight:479.571
Hs Code.:

Synonyms:(2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid

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Chemical Property of (2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid

Chemical Property:

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Technology Process of (2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid

There total 6 articles about (2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1623063-30-8
C₂₅H₃₇NO₇

: 1623063-20-6
(2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; In water; tert-butyl alcohol; at 0 ℃; for 4h;
DOI:10.1002/ejoc.201402430

Reference yield:

: 1623063-29-5
C₃₁H₄₇NO₇

: 1623063-20-6
(2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: camphor-10-sulfonic acid / methanol / 12 h / 0 - 20 °C

2.1: sodium periodate; cerium(III) chloride heptahydrate; ruthenium trichloride / water; acetonitrile; ethyl acetate / 0.08 h / 0 - 35 °C

2.2: 12 h / 0 °C

3.1: sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 4 h / 0 °C

With ruthenium trichloride; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; cerium(III) chloride heptahydrate; camphor-10-sulfonic acid; In methanol; water; ethyl acetate; acetonitrile; tert-butyl alcohol;
DOI:10.1002/ejoc.201402430

Reference yield:

: 1623063-16-0
(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

: 1623063-20-6
(2R,3R,4S)-4-[(2S,3R)-2-benzamido-3-hydroxybutanoyloxy]-2-butyl-3-(3-methylbutanoyloxy)pentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 0 °C

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 12 h / 0 - 20 °C

3.1: camphor-10-sulfonic acid / methanol / 12 h / 0 - 20 °C

4.1: sodium periodate; cerium(III) chloride heptahydrate; ruthenium trichloride / water; acetonitrile; ethyl acetate / 0.08 h / 0 - 35 °C

4.2: 12 h / 0 °C

5.1: sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 4 h / 0 °C

With ruthenium trichloride; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; cerium(III) chloride heptahydrate; camphor-10-sulfonic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1002/ejoc.201402430