(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

Base Information

Chemical Name:(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate
CAS No.:1623063-16-0
Molecular Formula:C₂₃H₃₆O₄
Molecular Weight:376.536
Hs Code.:

Synonyms:(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

Chemical Property:

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Technology Process of (2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

There total 3 articles about (2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1468-39-9
Isovaleric anhydride

: 1623063-15-9
(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-ol

: 1623063-16-0
(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.201402430

Reference yield:

: 218435-12-2
(2R)-2-[(4-methoxybenzyl)oxy]propanal

: 1623063-16-0
(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium bromide ethyl etherate / dichloromethane / -30 °C

2: pyridine; dmap / dichloromethane / 20 °C

With pyridine; dmap; magnesium bromide ethyl etherate; In dichloromethane;
DOI:10.1002/ejoc.201402430

Reference yield:

: 955948-60-4
(2R)-2-[(4-methoxybenzyl)oxy]propan-1-ol

: 1623063-16-0
(2R,3R,4S)-4-butyl-2-(4-methoxybenzyloxy)hexa-5-en-3-yl 3-methylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium hypochlorite / dichloromethane / 0 °C

2: magnesium bromide ethyl etherate / dichloromethane / -30 °C

3: pyridine; dmap / dichloromethane / 20 °C

With pyridine; dmap; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; magnesium bromide ethyl etherate; potassium bromide; In dichloromethane;
DOI:10.1002/ejoc.201402430