2-methyl-N⁴-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine

Base Information

• Chemical Name: 2-methyl-N⁴-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine
• CAS No.: 329943-39-7
• Molecular Formula: C₁₄H₂₃N₃
• Molecular Weight: 233.357
• Mol file: 329943-39-7.mol

Synonyms:2-methyl-N⁴-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine

Chemical Property of 2-methyl-N⁴-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-methyl-N⁴-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine

There total 3 articles about 2-methyl-N⁴-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-methyl-4-nitro-N-[3-(1-pyrrolidinyl)propyl]aniline (329943-37-5) → 2-methyl-N4-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine (329943-39-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 1h; under 2689.17 Torr;

DOI:10.1021/jm050670l

Reference yield:

3-(1-pyrrolidinyl)propylamine (23159-07-1) → 2-methyl-N4-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine (329943-39-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / aq. NaHCO₃; pyridine / 3 h / Heating

2: 99 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 2689.17 Torr

With pyridine; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol;

DOI:10.1021/jm050670l

Reference yield:

5-Fluoro-2-nitrotoluene (446-33-3) → 2-methyl-N4-[3-(1-pyrrolidinyl)propyl]-1,4-benzenediamine (329943-39-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / aq. NaHCO₃; pyridine / 3 h / Heating

2: 99 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 2689.17 Torr

With pyridine; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol;

DOI:10.1021/jm050670l

upstream raw materials:

3-methyl-4-nitro-N-[3-(1-pyrrolidinyl)propyl]aniline

3-(1-pyrrolidinyl)propylamine

5-Fluoro-2-nitrotoluene