Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside

Base Information

Chemical Name:Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside
CAS No.:161822-74-8
Molecular Formula:C₂₀H₂₅NO₈Se
Molecular Weight:486.38
Hs Code.:

Synonyms:Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside

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Technology Process of Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside

There total 5 articles about Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 150809-76-0
phenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-1-seleno-α-D-galactopyranoside

: 507-09-5
tiolacetic acid

: 161822-74-8
Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside

Guidance literature:: DOI:10.1021/ol006682c

Reference yield:

: 4098-06-0
triacetyl-D-galactal

: 161822-74-8
Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / NaN₃; PhI(OAc)2

2: 95 percent

With sodium azide; [bis(acetoxy)iodo]benzene; 1: Addition / 2: Reduction;
DOI:10.1021/ol006682c

Reference yield:

: 1666-13-3
diphenyl diselenide

: 161822-74-8
Phenyl 2-(N-acetylamino)-3,4,6-tri-O-acetyl-2-deoxy-1-seleno-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaN₃, (diacetoxyiodo)benzene / CH₂Cl₂ / 48 h / Ambient temperature

2: 1.) propanedithiol, Et₃N, 2.) pyridine / 1.) MeOH, r.t., 24 h

With pyridine; sodium azide; 1,2-propanedithiol; [bis(acetoxy)iodo]benzene; triethylamine; In dichloromethane;
DOI:10.1021/jo00105a051