1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene

Base Information

Chemical Name:1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene
CAS No.:1615250-65-1
Molecular Formula:C₁₉H₂₆N₄O₃
Molecular Weight:358.44
Hs Code.:

Synonyms:1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene

Chemical Property:

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Technology Process of 1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene

There total 3 articles about 1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1443231-58-0
N-(tert-butoxycarbonyl)-N’-(furanyl-2-methyl)thiourea

: 5840-09-5
4-amino-1-(N-ethylamino)benzene

: 1615250-65-1
1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene

Guidance literature:: With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1016/j.ejmech.2014.05.057

Reference yield:

: 145013-05-4
tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

: 1615250-65-1
1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride; trifluoroacetic anhydride / tetrahydrofuran; mineral oil / 18 h

2: mercury dichloride; triethylamine / dichloromethane / 15 h / 0 - 20 °C

With sodium hydride; triethylamine; trifluoroacetic anhydride; mercury dichloride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.ejmech.2014.05.057

Reference yield:

: 617-89-0
furan-2-ylmethanamine

: 1615250-65-1
1-[1-(tert-butoxycarbonyl)-3-(furan-2-ylmethyl)guanidino]-4-ethylaminobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride; trifluoroacetic anhydride / tetrahydrofuran; mineral oil / 18 h

2: mercury dichloride; triethylamine / dichloromethane / 15 h / 0 - 20 °C

With sodium hydride; triethylamine; trifluoroacetic anhydride; mercury dichloride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.ejmech.2014.05.057