2-dimethylgerma 1-phenyl phosphetane

Base Information

Chemical Name:2-dimethylgerma 1-phenyl phosphetane
CAS No.:78665-53-9
Molecular Formula:C₁₀H₁₅GeP
Molecular Weight:238.793
Hs Code.:

Synonyms:2-dimethylgerma 1-phenyl phosphetane

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Chemical Property of 2-dimethylgerma 1-phenyl phosphetane

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Technology Process of 2-dimethylgerma 1-phenyl phosphetane

There total 3 articles about 2-dimethylgerma 1-phenyl phosphetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 82312-13-8
1-(phenylphosphino)-2-(dimethylbromogermyl)ethane

: 78665-53-9
2-dimethylgerma 1-phenyl phosphetane

: 82312-20-7
2-(dimethyl-n-butylgermyl)-1-(phenylphosphino)ethane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; diethyl ether; byproducts: LiBr; n-C4H9Li soln. in Et2O added dropwise to Ge compd. soln. in THF; pentane added, centrifuged, solvent distd., oil distd.;

Reference yield:

: 82312-13-8
1-(phenylphosphino)-2-(dimethylbromogermyl)ethane

: 78665-53-9
2-dimethylgerma 1-phenyl phosphetane

: 68160-18-9
(CH₃)2GeP(C₆H₅)

: 81744-50-5
((CH₃)2GePC₆H₅)2CH₂CH₂

: 78665-55-1
trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

: 82312-28-5
3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane

Guidance literature:: With dimethyl amine; In benzene; byproducts: dimethylamine hydrobromide; Ge compd. soln. stirred at -30°C, 2-fold excess of dimethylamineallowed to bubble; centrifuged, evapd. (vac.), washed with C6H6, then with pentane, distd., obtained as mixt.;