trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

Base Information

Chemical Name:trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane
CAS No.:78665-55-1
Molecular Formula:C₁₆H₂₀GeP₂
Molecular Weight:346.872
Hs Code.:

Synonyms:trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

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Chemical Property of trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

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Technology Process of trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

There total 4 articles about trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 81744-50-5
((CH₃)2GePC₆H₅)2CH₂CH₂

: 624-92-0
Dimethyldisulphide

: 78665-55-1
trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

: 1767-35-7
bis(thiomethyl)dimethylgermanium

Guidance literature:: In neat (no solvent); educt heated at 150°C under 0.01 mmHg in flask connected to trapcooled at -196°C and filled with CH3SSCH3, reacted for 6 h; distd.;

Reference yield:

: 82312-13-8
1-(phenylphosphino)-2-(dimethylbromogermyl)ethane

: 78665-53-9
2-dimethylgerma 1-phenyl phosphetane

: 68160-18-9
(CH₃)2GeP(C₆H₅)

: 81744-50-5
((CH₃)2GePC₆H₅)2CH₂CH₂

: 78665-55-1
trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

: 82312-28-5
3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane

Guidance literature:: With dimethyl amine; In benzene; byproducts: dimethylamine hydrobromide; Ge compd. soln. stirred at -30°C, 2-fold excess of dimethylamineallowed to bubble; centrifuged, evapd. (vac.), washed with C6H6, then with pentane, distd., obtained as mixt.;