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3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane

Base Information
  • Chemical Name:3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane
  • CAS No.:82312-28-5
  • Molecular Formula:C18H26Ge2P2
  • Molecular Weight:449.532
  • Hs Code.:
3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane

Synonyms:3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane

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Chemical Property of 3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane
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Technology Process of 3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane

There total 1 articles about 3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dimethyl amine; In benzene; byproducts: dimethylamine hydrobromide; Ge compd. soln. stirred at -30°C, 2-fold excess of dimethylamineallowed to bubble; centrifuged, evapd. (vac.), washed with C6H6, then with pentane, distd., obtained as mixt.;
Guidance literature:
With lithium aluminium tetrahydride; In diethyl ether; LiAlH4 (2-fold excess) added in portions to educts mixt. in Et2O, refluxed for 6 h; hydrolyzed, extd. (Et2O), dried (Na2SO4), distd.; elem. anal.;
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