C₁₃H₁₃BrO₆

Base Information

• Chemical Name: C₁₃H₁₃BrO₆
• CAS No.: 1215090-31-5
• Molecular Formula: C₁₃H₁₃BrO₆
• Molecular Weight: 345.147
• Mol file: 1215090-31-5.mol

Synonyms:C₁₃H₁₃BrO₆

Chemical Property of C₁₃H₁₃BrO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₃BrO₆

There total 2 articles about C₁₃H₁₃BrO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

acetyl chloride (75-36-5) + 3,5-dihydroxy-4-bromobenzoic acid ethyl ester (350035-53-9) → C13H13BrO6 (1215090-31-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ja906162u

Reference yield:

3,5-dihydroxy-4-bromobenzoic acid (16534-12-6) → C13H13BrO6 (1215090-31-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid

2: triethylamine

With sulfuric acid; triethylamine;

DOI:10.1021/acs.langmuir.5b04540

Reference yield:

C13H13BrO6 (1215090-31-5) → C69H96O24 (1190085-90-5)

Guidance literature:

Multi-step reaction with 6 steps

1: bis-triphenylphosphine-palladium(II) chloride

2: lithium aluminium tetrahydride

5: Dowex

6: 18-crown-6 ether; potassium carbonate

With bis-triphenylphosphine-palladium(II) chloride; lithium aluminium tetrahydride; 18-crown-6 ether; potassium carbonate; 1: Stille coupling;

DOI:10.1002/anie.201006193

upstream raw materials:

acetyl chloride

3,5-dihydroxy-4-bromobenzoic acid ethyl ester

3,5-dihydroxy-4-bromobenzoic acid

Downstream raw materials:

C₆₉H₉₆O₂₄