Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

Base Information

Chemical Name:Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate
CAS No.:130082-85-8
Molecular Formula:C₂₄H₂₆O₂Se
Molecular Weight:425.429
Hs Code.:

Synonyms:Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

Suppliers and Price of Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

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Chemical Property of Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

Chemical Property:

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Technology Process of Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

There total 8 articles about Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130082-81-4
cis-Hexahydro-7a-(3-phenyl-2-propynyl)-1(3H)-isobenzofuranone

: 130082-85-8
Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / 1.) THF, reflux, 50 min, 2.) THF, HMPA, reflux, 4 h

2: diethyl ether

With sodium hydride; In diethyl ether;
DOI:10.1021/jo00076a057

Reference yield:

: 6939-71-5
hexahydro-isobenzo[c]furan-1-one

: 130082-85-8
Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / LDA / tetrahydrofuran; hexane / 1.) -78 deg C, 40 min, 2.) r.t., overnight

2: NaH / 1.) THF, reflux, 50 min, 2.) THF, HMPA, reflux, 4 h

3: diethyl ether

With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jo00076a057

Reference yield:

: 1794-48-5
1-bromo-3-phenylprop-2-yne

: 130082-85-8
Methyl cis-1-(3-phenyl-2-propynyl)-2-<(phenylseleno)methyl>cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / LDA / tetrahydrofuran; hexane / 1.) -78 deg C, 40 min, 2.) r.t., overnight

2: NaH / 1.) THF, reflux, 50 min, 2.) THF, HMPA, reflux, 4 h

3: diethyl ether

With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jo00076a057