tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate

Base Information

Chemical Name:tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate
CAS No.:1238895-31-2
Molecular Formula:C₂₂H₃₇NO₃Si
Molecular Weight:391.626
Hs Code.:

Synonyms:tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate

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Chemical Property of tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate

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Technology Process of tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate

There total 1 articles about tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1238895-00-5
(2R)-2-{[(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-en-1-yl]amino}-2-phenylethanol

: 1238895-31-2
tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate

Guidance literature:: (2R)-2-{[(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-en-1-yl]amino}-2-phenylethanol; With methanol; lead(IV) tetraacetate; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

With hydroxylamine hydrochloride; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

di-tert-butyl dicarbonate; With triethylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201000255

Reference yield: 68.0%

: 1238895-31-2
tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate

: 1238895-36-7
tert-butyl (2R,3S)-3-[(tert-butyldimethylsilyloxy)methyl]-2-phenylpyrrolidine-1-carboxylate

Guidance literature:: tert-butyl [(1R,2S)-2-[(tert-butyldimethylsilyloxy)methyl]-1-phenylbut-3-enyl]carbamate; With Schwartz's reagent; In dichloromethane; Inert atmosphere;

With iodine; In dichloromethane; for 2h; Inert atmosphere;

With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201000255