1,3-DIMETHYL-5-([4-(METHYLSULFANYL)PHENYL]METHYLENE)-2,4,6(1H,3H,5H)-PYRIMIDINETRIONE

Base Information

• Chemical Name: 1,3-DIMETHYL-5-([4-(METHYLSULFANYL)PHENYL]METHYLENE)-2,4,6(1H,3H,5H)-PYRIMIDINETRIONE
• CAS No.: 444151-79-5
• Molecular Formula: C₁₄H₁₄N₂O₃S
• Molecular Weight: 290.343
• Mol file: 444151-79-5.mol

Synonyms:1,3-dimethyl-5-[4-(methylsulfanyl)benzylidene]-2,4,6(1H,3H,5H)pyrimidinetrione

Chemical Property of 1,3-DIMETHYL-5-([4-(METHYLSULFANYL)PHENYL]METHYLENE)-2,4,6(1H,3H,5H)-PYRIMIDINETRIONE

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

1,3-DIMETHYL-5-((4-(METHYLSULFANYL)PHENYL)METHYLENE)-2,4,6(1H,3H,5H)-PYRIMIDINETRIONE 95.00% ^*data from reagent suppliers

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Technology Process of 1,3-DIMETHYL-5-([4-(METHYLSULFANYL)PHENYL]METHYLENE)-2,4,6(1H,3H,5H)-PYRIMIDINETRIONE

There total 1 articles about 1,3-DIMETHYL-5-([4-(METHYLSULFANYL)PHENYL]METHYLENE)-2,4,6(1H,3H,5H)-PYRIMIDINETRIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,3-dimethylbarbituric acid (769-42-6) + 4-(Methylthio)benzaldehyde (3446-89-7) → 1,3-dimethyl-5-[4-(methylsulfanyl)benzylidene]-2,4,6(1H,3H,5H)pyrimidinetrione (444151-79-5)

Guidance literature:

In water; at 100 ℃; for 0.5h;

DOI:10.2174/157340611795564231

Reference yield: 55.0%

1-Phenyl-3-methyl-5-aminopyrazole (1131-18-6) + 1,3-dimethyl-5-[4-(methylsulfanyl)benzylidene]-2,4,6(1H,3H,5H)pyrimidinetrione (444151-79-5) + 4-methoxy-benzaldehyde (123-11-5) → 6-(4-methoxyphenyl)-1',3,3'-trimethyl-4-[4-(methylsulfanyl)phenyl]-1-phenyl-1,4,6,7-tetrahydro-2'H-spiro[pyrazolo[3,4-b]pyridine-5,5'-pyrimidine]-2',4',6'(1'H,3'H)-trione (1172135-18-0)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 3h; chemoselective reaction; Sonication;

DOI:10.1055/s-0028-1088024

upstream raw materials:

1,3-dimethylbarbituric acid

4-(Methylthio)benzaldehyde

Downstream raw materials:

6-(4-methoxyphenyl)-1',3,3'-trimethyl-4-[4-(methylsulfanyl)phenyl]-1-phenyl-1,4,6,7-tetrahydro-2'H-spiro[pyrazolo[3,4-b]pyridine-5,5'-pyrimidine]-2',4',6'(1'H,3'H)-trione

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