(5'S,8R)-N-benzoyl-O₃'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine

Base Information

• Chemical Name: (5'S,8R)-N-benzoyl-O₃'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine
• CAS No.: 898253-81-1
• Molecular Formula: C₂₃H₃₁N₅O₄Si
• Molecular Weight: 469.616

Synonyms:(5'S,8R)-N-benzoyl-O₃'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine

Chemical Property of (5'S,8R)-N-benzoyl-O₃'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of (5'S,8R)-N-benzoyl-O₃'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine

There total 1 articles about (5'S,8R)-N-benzoyl-O₃'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5'-aldehyde-2'-deoxy-6-N-benzoyl-3'-O-tertbutyldimethylsilyl adenosine (167700-45-0) → (5'S,8R)-N-benzoyl-O3'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine (898253-81-1) + 6-N-benzoyl-3'-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine (51549-40-7) + (5?'S)-N6-benzoyl-3?'-O-(tert-butyldimethylsilyl)-5?',8-cyclo-2?'-deoxyadenosine (211919-88-9)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In fluorobenzene; for 2h; Heating;

DOI:10.1021/jo060197z

Reference yield: 100.0%

(5'S,8R)-N-benzoyl-O3'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine (898253-81-1) → (5?'S)-N6-benzoyl-3?'-O-(tert-butyldimethylsilyl)-5?',8-cyclo-2?'-deoxyadenosine (211919-88-9)

Guidance literature:

With air; In chloroform;

DOI:10.1021/jo060197z

Reference yield: 90.0%

(5'S,8R)-N-benzoyl-O3'-(tert-butyldimethylsilyl)-5',8-cyclo-7,8-dihydro-2'-deoxyadenosine (898253-81-1) → N6-benzoyl-3'-O-(tert-butyldimethylsilyl)-5',8-cyclo-5'-oxo-2'-deoxyadenosine (211919-87-8)

Guidance literature:

With chloranil; In o-xylene; for 0.333333h; Heating;

DOI:10.1021/jo060197z

upstream raw materials:

5'-aldehyde-2'-deoxy-6-N-benzoyl-3'-O-tertbutyldimethylsilyl adenosine

Downstream raw materials:

(5?'S)-N⁶-benzoyl-3?'-O-(tert-butyldimethylsilyl)-5?',8-cyclo-2?'-deoxyadenosine

N⁶-benzoyl-3'-O-(tert-butyldimethylsilyl)-5',8-cyclo-5'-oxo-2'-deoxyadenosine

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