2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde

Base Information

Chemical Name:2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde
CAS No.:938071-28-4
Molecular Formula:C₂₀H₂₇NO₄Si
Molecular Weight:373.524
Hs Code.:

Synonyms:2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde

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Chemical Property of 2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde

Chemical Property:

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Technology Process of 2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde

There total 6 articles about 2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 938071-31-9
[2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazol-4-yl]methanol

: 938071-28-4
2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane;
DOI:10.1039/b618160k

Reference yield:

: 3-hydroxy-4-methoxycinnamamide

: 938071-28-4
2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / imidazole / dimethylformamide

2: 90 percent / dirhodium tetraacetate / CH₂Cl₂ / 4 h / Heating

3: 81 percent / triethylamine; triphenylphosphine; iodine / CH₂Cl₂ / 20 °C

4: 93 percent / DIBAL / CH₂Cl₂

5: 92 percent / Dess-Martin periodinane / CH₂Cl₂

With 1H-imidazole; iodine; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; triphenylphosphine; dirhodium tetraacetate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b618160k

Reference yield:

: 938071-25-1
(E)-3-(3-tert-butyldimethylsiloxy-4-methoxyphenyl)acrylamide

: 938071-28-4
2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / dirhodium tetraacetate / CH₂Cl₂ / 4 h / Heating

2: 81 percent / triethylamine; triphenylphosphine; iodine / CH₂Cl₂ / 20 °C

3: 93 percent / DIBAL / CH₂Cl₂

4: 92 percent / Dess-Martin periodinane / CH₂Cl₂

With iodine; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; triphenylphosphine; dirhodium tetraacetate; In dichloromethane;
DOI:10.1039/b618160k