methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate

Base Information

Chemical Name:methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate
CAS No.:938071-27-3
Molecular Formula:C₂₁H₂₉NO₅Si
Molecular Weight:403.55
Hs Code.:

Synonyms:methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate

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Chemical Property of methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate

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Technology Process of methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate

There total 5 articles about methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 938071-26-2
(E)-methyl 2-[(3-tert-butyldimethylsilyloxy-4-methoxyphenyl)propenoylamino]-3-oxobutanoate

: 938071-27-3
methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate

Guidance literature:: With iodine; triethylamine; triphenylphosphine; In dichloromethane; at 20 ℃;
DOI:10.1039/b618160k

Reference yield: 41.0%

: 24762-04-7
2-Diazo-3-oxo-butyric acid methyl ester

: 1096163-98-2
(E)-3-(3-tert-butyldimethylsiloxy-4-methoxyphenyl)acrylonitrile

: 938071-27-3
methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate

Guidance literature:: With dirhodium tetraacetate; In dichloromethane; for 16h; Reflux; Inert atmosphere;
DOI:10.1039/b810855b

Reference yield:

: 3-hydroxy-4-methoxycinnamamide

: 938071-27-3
methyl 2-(3-tert-butyldimethylsilyloxy-4-methoxystyryl)-5-methyloxazole-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / imidazole / dimethylformamide

2: 90 percent / dirhodium tetraacetate / CH₂Cl₂ / 4 h / Heating

3: 81 percent / triethylamine; triphenylphosphine; iodine / CH₂Cl₂ / 20 °C

With 1H-imidazole; iodine; triethylamine; triphenylphosphine; dirhodium tetraacetate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b618160k