C₅₂H₇₀N₁₀O₁₆S

Base Information

Chemical Name:C₅₂H₇₀N₁₀O₁₆S
CAS No.:1346444-95-8
Molecular Formula:C₅₂H₇₀N₁₀O₁₆S
Molecular Weight:1123.25
Hs Code.:

C<sub>52</sub>H<sub>70</sub>N<sub>10</sub>O<sub>16</sub>S

Synonyms:C₅₂H₇₀N₁₀O₁₆S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₇₀N₁₀O₁₆S

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Technology Process of C₅₂H₇₀N₁₀O₁₆S

There total 23 articles about C₅₂H₇₀N₁₀O₁₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: C₆₆H₈₂N₁₀O₁₆S

: 1346444-95-8
C₅₂H₇₀N₁₀O₁₆S

Guidance literature:: With trimethylsilyl bromide; methyl-phenyl-thioether; 3-methyl-phenol; trifluoroacetic acid; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.062

Reference yield:

: 1346444-74-3
N'-(2-phenylsulfonylacetyl)hydrazinecarboxylic acid tert-butyl ester

: 1346444-95-8
C₅₂H₇₀N₁₀O₁₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: piperidine; acetic acid / toluene / 18 h / Inert atmosphere; Reflux

2.1: trifluoroacetic acid / 1.5 h / 0 °C / Inert atmosphere

2.2: 0.05 h / Inert atmosphere

3.1: benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / 1.5 h / 0 °C / Inert atmosphere

4.2: 0.05 h / 0 °C / Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

6.1: trimethylsilyl bromide; methyl-phenyl-thioether; 3-methyl-phenol; trifluoroacetic acid / 1.5 h / 0 °C / Inert atmosphere

With piperidine; trimethylsilyl bromide; methyl-phenyl-thioether; benzotriazol-1-ol; acetic acid; 3-methyl-phenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide; toluene; 1.1: Knoevenagel condensation;
DOI:10.1016/j.tet.2011.09.062

Reference yield:

: 1346444-76-5
N'-{2-benzenesulfonyl-3-[2,4-dimethyl-6-(2-nitrobenzyloxy)phenyl]-(E)-acryloyl}hydrazinecarboxylic acid tert-butyl ester

: 1346444-95-8
C₅₂H₇₀N₁₀O₁₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / 1.5 h / 0 °C / Inert atmosphere

1.2: 0.05 h / Inert atmosphere

2.1: benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / 1.5 h / 0 °C / Inert atmosphere

3.2: 0.05 h / 0 °C / Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

5.1: trimethylsilyl bromide; methyl-phenyl-thioether; 3-methyl-phenol; trifluoroacetic acid / 1.5 h / 0 °C / Inert atmosphere

With trimethylsilyl bromide; methyl-phenyl-thioether; benzotriazol-1-ol; 3-methyl-phenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.062