(4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate

Base Information

Chemical Name:(4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate
CAS No.:187851-96-3
Molecular Formula:C₁₄H₂₀O₅
Molecular Weight:268.31
Hs Code.:

Synonyms:(4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate

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Technology Process of (4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate

There total 4 articles about (4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 187851-95-2
(4-methoxyphenyl)methyl hex-5-enoate

: 187851-96-3
(4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate

: 213532-96-8
(S)-5,6-Dihydroxy-hexanoic acid 4-methoxy-benzyl ester

Guidance literature:: With potassium osmate(VI); 1,4-bis(dihydroquinidinyl)anthraquinone; water; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III); In tert-butyl alcohol; at 0 ℃; for 12h; Yields of byproduct given;
DOI:10.1055/s-1998-2123

Reference yield: 51.0%

: 187851-95-2
(4-methoxyphenyl)methyl hex-5-enoate

: 187851-96-3
(4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate

Guidance literature:: With (DHQD)2AQN; K₂OsO₂(OH)2; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III); In tert-butyl alcohol; at 0 ℃; for 48h;
DOI:10.1021/jo962166h

Reference yield:

: 1577-22-6
5-hexenoic acid

: 187851-96-3
(4-methoxyphenyl)methyl (R)-5,6-dihydroxyhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NaHCO₃ / dimethylformamide / 72 h / 45 °C

2: 51 percent / K₃Fe(CN)6, K₂CO₃, NaHCO₃, (DHQD)2-AQN, K₂OsO₂(OH)2 / 2-methyl-propan-2-ol / 48 h / 0 °C

With (DHQD)2AQN; K₂OsO₂(OH)2; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III); In N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jo962166h