2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide

Base Information

Chemical Name:2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide
CAS No.:1429764-32-8
Molecular Formula:C₁₉H₁₇BrN₂O₄S₂
Molecular Weight:481.391
Hs Code.:

Synonyms:2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide

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Chemical Property of 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide

Chemical Property:

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Technology Process of 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide

There total 5 articles about 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1429764-30-6
methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

: 1429764-32-8
2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide

Guidance literature:: With ammonium hydroxide; In water; at 20 ℃; for 1h;
DOI:10.1021/jm500010b

Reference yield:

: 4900-63-4
1-methoxy-4-nitronaphthalene

: 1429764-32-8
2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-iodo-succinimide; trifluoroacetic acid / 20 h / Reflux; Inert atmosphere

2.1: zinc(II) chloride; caesium carbonate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2.2: 20 h / 60 °C / Inert atmosphere

3.1: iron; acetic acid / 1 h / 70 °C

3.2: 20 °C

4.1: ammonium hydroxide / water / 1 h / 20 °C

With ammonium hydroxide; N-iodo-succinimide; iron; caesium carbonate; acetic acid; trifluoroacetic acid; zinc(II) chloride; In tetrahydrofuran; water;

Reference yield:

: 1429765-70-7
2-iodo-1-methoxy-4-nitronaphthalene

: 1429764-32-8
2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc(II) chloride; caesium carbonate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

1.2: 20 h / 60 °C / Inert atmosphere

2.1: iron; acetic acid / 1 h / 70 °C

2.2: 20 °C

3.1: ammonium hydroxide / water / 1 h / 20 °C

With ammonium hydroxide; iron; caesium carbonate; acetic acid; zinc(II) chloride; In tetrahydrofuran; water;