methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

Base Information

Chemical Name:methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?
CAS No.:1429764-30-6
Molecular Formula:C₂₀H₁₈BrNO₅S₂
Molecular Weight:496.403
Hs Code.:

Synonyms:methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

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Chemical Property of methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

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Technology Process of methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

There total 6 articles about methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate? which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1429765-71-8
methyl 2-((1-methoxy-4-nitronaphthalen-2-yl)thio)acetate

: 98-58-8
4-bromobenzenesulfonyl chloride

: 1429764-30-6
methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

Guidance literature:: methyl 2-((1-methoxy-4-nitronaphthalen-2-yl)thio)acetate; With iron; acetic acid; at 70 ℃; for 1h;

4-bromobenzenesulfonyl chloride; With pyridine; In dichloromethane; at 20 ℃;

Reference yield:

: 1429765-78-5
methyl 2-((4-amino-1-methoxynaphthalen-2-yl)thio)acetate

: 98-58-8
4-bromobenzenesulfonyl chloride

: 1429764-30-6
methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm500010b

Reference yield:

: 4900-63-4
1-methoxy-4-nitronaphthalene

: 1429764-30-6
methyl 2-((4-(4-bromophenylsulfonamido)-1-methoxynaphthalen-2-yl)thio)acetate?

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-iodo-succinimide; trifluoroacetic acid / 20 h / Reflux; Inert atmosphere

2.1: zinc(II) chloride; caesium carbonate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2.2: 20 h / 60 °C / Inert atmosphere

3.1: iron; acetic acid / 1 h / 70 °C

3.2: 20 °C

With N-iodo-succinimide; iron; caesium carbonate; acetic acid; trifluoroacetic acid; zinc(II) chloride; In tetrahydrofuran;