8-benzenesulfonyloxy-2-bromomethylquinoline

Base Information

Chemical Name:8-benzenesulfonyloxy-2-bromomethylquinoline
CAS No.:213881-32-4
Molecular Formula:C₁₆H₁₂BrNO₃S
Molecular Weight:378.246
Hs Code.:

Synonyms:8-benzenesulfonyloxy-2-bromomethylquinoline

Suppliers and Price of 8-benzenesulfonyloxy-2-bromomethylquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-benzenesulfonyloxy-2-bromomethylquinoline

Chemical Property:

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Technology Process of 8-benzenesulfonyloxy-2-bromomethylquinoline

There total 3 articles about 8-benzenesulfonyloxy-2-bromomethylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 213881-38-0
2-methylquinolin-8-yl benzenesulfonate

: 213881-32-4
8-benzenesulfonyloxy-2-bromomethylquinoline

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 2.5h; Heating;
DOI:10.1021/jo980563h

Reference yield:

: 826-81-3
2-methyl-8-quinolinol

: 213881-32-4
8-benzenesulfonyloxy-2-bromomethylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 1.5 h / 0 - 20 °C

2: 60 percent / NBS, AIBN / CCl₄ / 2.5 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1021/jo980563h

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 213881-32-4
8-benzenesulfonyloxy-2-bromomethylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 1.5 h / 0 - 20 °C

2: 60 percent / NBS, AIBN / CCl₄ / 2.5 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1021/jo980563h