2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate

Base Information

Chemical Name:2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate
CAS No.:1610763-29-5
Molecular Formula:C₃₃H₃₁NO₅
Molecular Weight:521.613
Hs Code.:

Synonyms:2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate

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Chemical Property of 2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate

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Technology Process of 2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate

There total 9 articles about 2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7451-98-1
3',4'-dihydroxypropiophenone

: 1610763-29-5
2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: Reflux

2.1: acetic acid; bromine / 0.5 h / 20 °C

3.1: triethylamine / ethanol / 16 h / 80 °C / Inert atmosphere

3.2: 14 h / 115 °C / Inert atmosphere; Sealed tube

4.1: caesium carbonate / acetone / 20 h / 60 °C

With bromine; potassium carbonate; caesium carbonate; acetic acid; triethylamine; In ethanol; acetone; 3.1: |Bischler-Moehlau Indole Synthesis / 3.2: |Bischler-Moehlau Indole Synthesis;
DOI:10.1021/jm500351m

Reference yield:

: 17269-65-7
1-(3,4-bis(benzyloxy)phenyl)propan-1-one

: 1610763-29-5
2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; bromine / 0.5 h / 20 °C

2.1: triethylamine / ethanol / 16 h / 80 °C / Inert atmosphere

2.2: 14 h / 115 °C / Inert atmosphere; Sealed tube

3.1: caesium carbonate / acetone / 20 h / 60 °C

With bromine; caesium carbonate; acetic acid; triethylamine; In ethanol; acetone; 2.1: |Bischler-Moehlau Indole Synthesis / 2.2: |Bischler-Moehlau Indole Synthesis;
DOI:10.1021/jm500351m

Reference yield:

: 17518-01-3
1-(3,4-bis(benzyloxy)phenyl)-2-bromopropan-1-one

: 1610763-29-5
2-((2-(3,4-bis(benzyloxy)phenyl)-3-methyl-1H-indol-5-yl)oxy)ethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / ethanol / 16 h / 80 °C / Inert atmosphere

1.2: 14 h / 115 °C / Inert atmosphere; Sealed tube

2.1: caesium carbonate / acetone / 20 h / 60 °C

With caesium carbonate; triethylamine; In ethanol; acetone; 1.1: |Bischler-Moehlau Indole Synthesis / 1.2: |Bischler-Moehlau Indole Synthesis;
DOI:10.1021/jm500351m