1-[3,4-Bis(benzyloxy)phenyl]-2-bromopropan-1-one

Base Information

Chemical Name:1-[3,4-Bis(benzyloxy)phenyl]-2-bromopropan-1-one
CAS No.:17518-01-3
Molecular Formula:C23H21BrO3
Molecular Weight:425.31500
Hs Code.:
DSSTox Substance ID:DTXSID30512868

Synonyms:17518-01-3;1-[3,4-Bis(benzyloxy)phenyl]-2-bromopropan-1-one;SCHEMBL5893913;DTXSID30512868

Suppliers and Price of 1-[3,4-Bis(benzyloxy)phenyl]-2-bromopropan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3,4-Bis(benzyloxy)phenyl]-2-bromopropan-1-one

Chemical Property:

PSA：35.53000
LogP:5.81070
XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:8
Exact Mass:424.06741
Heavy Atom Count:27
Complexity:443

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C(=O)C1=CC(=C(C=C1)OCC2=CC=CC=C2)OCC3=CC=CC=C3)Br

Technology Process of 1-[3,4-Bis(benzyloxy)phenyl]-2-bromopropan-1-one

There total 5 articles about 1-[3,4-Bis(benzyloxy)phenyl]-2-bromopropan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 17269-65-7
1-(3,4-bis(benzyloxy)phenyl)propan-1-one

: 17518-01-3
1-(3,4-bis(benzyloxy)phenyl)-2-bromopropan-1-one

Guidance literature:: With bromine; acetic acid; at 20 ℃; for 0.5h;
DOI:10.1021/jm500351m

Reference yield:

: 7451-98-1
3',4'-dihydroxypropiophenone

: 17518-01-3
1-(3,4-bis(benzyloxy)phenyl)-2-bromopropan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: Reflux

2.1: acetic acid; bromine / 0.5 h / 20 °C

With bromine; potassium carbonate; acetic acid; In acetone;
DOI:10.1021/jm500351m

Reference yield:

: 100-39-0
benzyl bromide

: 17518-01-3
1-(3,4-bis(benzyloxy)phenyl)-2-bromopropan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: Reflux

2.1: acetic acid; bromine / 0.5 h / 20 °C

With bromine; potassium carbonate; acetic acid; In acetone;
DOI:10.1021/jm500351m