benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate

Base Information

Chemical Name:benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate
CAS No.:128984-21-4
Molecular Formula:C₁₅H₂₀NO₆P
Molecular Weight:341.301
Hs Code.:

benzyl DL-5-<ethoxy(methyl)phosphinyl>-2-oxotetrahydrofuran-3-ylcarbamate

Synonyms:benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate

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Chemical Property of benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate

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Technology Process of benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate

There total 5 articles about benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 115220-67-2,115268-19-4,129097-29-6
benzyl DL-N-benzyloxycarbonyl-4-homoserinate

: 128984-21-4
benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 23 ℃;
DOI:10.1039/c39870001710

Reference yield:

: 31332-88-4
(S)-3-(N-benzyloxycarbonylamino)tetrahydrofuran-2-one

: 128984-21-4
benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaOH / methanol; dimethylformamide / 24 h / 23 °C

2: 100 percent / oxalyl chloride, Et₃N / dimethylsulfoxide; CH₂Cl₂ / -78 °C

3: 27 percent / CH₂Cl₂ / 23 °C

4: 100 percent / CF₃COOH / CH₂Cl₂ / 23 °C

With sodium hydroxide; oxalyl dichloride; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c39870001710

Reference yield:

: 58641-56-8
2-BENZYLOXYCARBONYLAMINO-4-OXO-BUTYRIC ACID BENZYL ESTER

: 128984-21-4
benzyl DL-5--2-oxotetrahydrofuran-3-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / CH₂Cl₂ / 23 °C

2: 100 percent / CF₃COOH / CH₂Cl₂ / 23 °C

With trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c39870001710